Recommended Values of ²³⁹Pu, ²⁴⁰Pu and ^239+240Pu Concentrations in Reference Material IAEA-315 (Marine Sediment) Estimated by Thermal Ionisation Mass Spectrometry, Inductively Coupled Plasma-Mass Spectrometry and Alpha Spectrometry     

Taeko Shinonaga  Helmuth Aigner  Dilani Klose  Peter Spinder  Heinz Fröschl  David Donohue 《Geostandards and Geoanalytical Research》2008,32(1):93-101

The recommended concentrations of ²³⁹Pu, ²⁴⁰Pu and ^239+240Pu in reference material IAEA‐315 (marine sediment) were estimated by three analytical methods: isotope dilution thermal ionisation mass spectrometry (TIMS), isotope dilution inductively coupled plasma‐mass spectrometry (ICP‐MS) and alpha spectrometry. The determination of ²³⁹Pu and ²⁴⁰Pu (^239+240Pu by alpha spectrometry) was carried out with samples from randomly selected bottles using each method. Plutonium‐238 was also measured by alpha spectrometry. A plutonium‐242 reference material was used as a spike for the quantitative analysis. The influence of ²⁴²Pu in the samples was therefore calculated; however, this contribution was less than the range of uncertainty and did not influence the final results. The obtained data were statistically analysed using variance component analysis and paired comparison. The combined standard uncertainties from “method/measurement”, “bottle” and “sub‐sample” were in the order of 3 to 6%. The main contributions to the uncertainty were from the material heterogeneity and from systematic differences between methods. Based on this study with twenty‐seven analyses using 10–14 g sample mass, concentrations of (38 ± 3) Bq kg^?1, (28 ± 3) Bq kg^?1 and (66 ± 4) Bq kg^?1 are proposed as recommended values for ²³⁹Pu, ²⁴⁰Pu and ^239+240Pu, respectively, and (9.5 ± 0.4) Bq kg^?1 for ²³⁸Pu as an information value in reference material IAEA‐315. In mass concentration units, these amount to (16.4 ± 1.2) ng kg^?1, (3.3 ± 0.4) ng kg^?1 and (0.015 ± 0.003) ng kg^?1 for ²³⁹Pu, ²⁴⁰Pu and ²³⁸Pu, respectively. The certified reference materials NIST 4350B and NIST 4354 were also analysed by TIMS for quality assurance of the method used in this study.  相似文献   

应用GPS数据与重力数据确定大地水准面     

于小平  张廷玉  刘财  陈增宝  许惠平  庞贺民 《吉林大学学报(地球科学版)》2008,38(5)

作为GPS/重力边值问题理论及方法的应用,在对GPS/重力方法确定(似)大地水准面的原理进行简要介绍与分析的基础上,利用收集到的N区的600个GPS/重力数据和48个高精度GPS水准数据,计算出该区域的(似)大地水准面。通过拟合法和系统差直接改正法进行的精度分析表明,应用GPS/重力数据结合水准方法确定的该地区(似)大地水准面的精度达到厘米级精度。  相似文献   

上海市建设用地勘测定界若干问题探讨     

周金龙 《上海国土资源》2008,(1):40-43

对在上海市建设用地勘测定界过程中涉及的土地权属界线认定、原土地用途划分时所现的若干问题进行了详细探讨,同时从政策角度、技术角度提出了以上问题的相应解决途径。  相似文献   

上海市长江口及邻近海域地质调查现状及展望   总被引：1，自引：1，他引：0  

谢建磊  王寒梅  何中发  李晓  黎兵 《上海国土资源》2008,(4)

海洋区域地质调查近年来逐渐得到重视,海洋地质调查技术的发展也为开展海洋区域地质调查奠定了基础。上海地区社会经济发展对地质工作的需求,为摸清上海市长江口及邻近海域的地质现状提出了必然要求。本文在系统整理长江口及邻近海域地质资料的基础上,重点分析了区内存在的重点地质问题和研究存在的问题,根据海洋地质调查的技术发展,结合国内相关地区的调查经验,对长江口及邻近海域内区域地质调查进行了展望,提出了采用综合物探技术、地质取样和测试分析进行综合地质环境调查的建议,并对具体采用的调查技术和调查内容进行了论述。  相似文献   

Extreme value analysis of diamond-size distributions     

J. Caers  P. Vynckier  J. Beirlant  L. Rombouts 《Mathematical Geology》1996,28(1):25-43

Extreme value analysis provides a semiparametric method for analyzing the extreme long tails of skew distributions which may be observed when handling mining data. The estimation of important tail characteristics, such as the extreme value index, allows for a discrimination between competing distribution models. It measures the thickness of such long tailed distributions, if only a limited sample is available. This paper stresses the practical implementation of extreme value theory, which is used to discriminate a lognormal from a mixed lognormal distribution in a case study of size distributions for alluvial diamonds.  相似文献   

CSU－RAMS模式在区域气侯模拟中的应用   总被引：1，自引：0，他引：1  

万齐林  施永年 《热带气象学报》1996,(2)

将ＣＳＵ－ＲＡＭＳ（中尺度）数值模式改造成“区域气候数值模式”以及进行区域气候数值模拟的试验研究。说明将有限区域中尺度数值模式与ＧＣＭ模式嵌套应用到区域气候数值模拟研究上能够取得有意义的结果。它能在一定程度上改善ＧＣＭ模式的不足。可以更为细致地描述大气环流的变化特征,是了解区域气候变化的有效方法之一。  相似文献   

The propagation of a single shear crack: A displacement discontinuity model     

J. -Cl. De Bremaecker  K. Wei 《Pure and Applied Geophysics》1994,142(3-4):567-585

Numerical studies using the displacement discontinuity method show that a single shear crack under compression propagates in its own direction, because such propagation results in the maximum release of strain energy. The methods of linear elastic fracture mechanics may not be used for such a closed crack, and the stress intensity factors are meaningless in that case. Laboratory observations of propagation by means of kinks at an angle of approximately 70° to the crack may be due to heterogeneities, to the effect of a preexisting crack, to end effects, to microcracking, or to some combination of these factors. Such kinks may thus be local phenomena which cannot release most of the strain energy, and are not incompatible with our numerical results which are based on a global energy balance.  相似文献   

华南二叠－三叠系的事件地层与生物地层界线   总被引：10，自引：1，他引：9  

王成源 《地层学杂志》1994,18(2):110-118,145

华南二叠－三叠系界线研究应严格区分事件地层界线与生物地层界线。“界线粘土”层的底界即为事件地层界线。生物地层界线定义不能与“混生层”或“过渡层”的概念连在一起。长兴煤山忠心大队剖面是最好的二叠－三叠系全球界线层型剖面点（ＧＳＳＰ）。二叠－三叠系生物地层界线定义为ＨｉｎｄｅｏｄｕｓｐａｒｖｕｓＭｏｒｐｈｏｔｙｐｅ１的首次出现,其位置就在长兴剖面界线层（混生层）２的内部,比事件地层界线高１５ｃｍ。ＨｉｎｄｅｏｄｕｓｐａｒｖｕｓＭｏｒｐｈｏｔｙｐｅ１的首次出现,即为长兴阶的顶界。  相似文献   

浙闽山区茶叶生产基地评价的探讨   总被引：6，自引：0，他引：6  

华熙成 《地理研究》1994,13(3):98-103

茶叶基地的评价包括对基地的自然和经济条件的评估,应用系统分析方法,将自然和经济条件进行定量的综合评估,用综合评价值区分基地间的差异,最后定性与定量相结合,提出茶叶生产基地的合理布局.  相似文献   

云南兰坪-思茅盆地生物地球化学找钾技术方法研究初探     

伯英  刘成林  沈力建  丁婷 《地质学报》2022,96(7):2626-2633

在生物地球化学和“深穿透”理论的指导下,在兰坪-思茅盆地勐野井钾盐矿区及周边开展了生物地球化学找钾技术方法的探索性研究。沿江城县勐野井钾盐矿区及周边一线,对乔木类植物叶子进行了取样,分析,数据处理,特征指标筛选,获得了研究区植物样品主量和微量组分含量背景值,初步圈定了异常区,与以往圈定的找钾远景区较吻合。该区生物地球化学找钾技术取得较好的效果,今后还需扩大采样区域,获得更多样本数据,将找钾特征指标及其异常值的阈值进一步补充完善。  相似文献